Singapore Journal of Scientific Research2010-006x2010-0051Science International10.3923/sjsres.2012.47.53Kigelia pinnata Leaves]]>AtolaniOlubunmi OladoyeSunday OluyoriA.P. OlatunjiA. Gabriel 2201222Kigelia pinnata (Lam) Benth is renowned for its traditional applications as anti-inflammatory, antioxidant, anti-microbial and anti-cancer effects. The leaves of Kigelia pinnata were extracted successively with hexane and ethylacetate at room temperature and the extracts fractionated on an open silica gel column using hexane, ethylacetate and methanol gradient of increasing polarity. Preparative thin layer chromatography was used for further purification and isolation of various compounds. Spectroscopic analyses from UV/VIS, IR, GC/GCMS, 1HNMR, 13CNMR, COSY and HETCOR techniques were used for the characterization of the compounds isolated from the leaves of Kigelia pinnata. The compound identification was based on spectral data comparison with literature data. Based on the data available to us, we report for the first time isolation of Hentriacontane, β-tocopherol, 3-hydro-4,8-phytene, trans-phytol, (9Z,12Z)-methyl octadeca-9, 12-dienoate and 1,3,3,5,6,6-hexamethylcyclohexa-1,4-diene from Kigelia pinnata leave.]]>Aires-de-Sousa, J., M.C. Hemmer and J. Gasteiger,2002748090Akah, P.A.,199643138Atolani, O., A.G. Olatunji, O.S. Adeyemi and O.S. Fayemi,2009Kigelia africana.]]>34187194Azu, O.O., F.I.O. Duru, A.A. Osinubi, A.A. Oremosu, C.C. Norohna, A.O. Okanlawon and S.O. Elesha,2011Kigelia pinnata fruit extract ameliorates the testicular toxicity following cisplatin administration in male Sprague-Dawley rats.]]>5388397Burkill, H.M.,1985Vol. 1.pp: 254-257pp: 254-257Dauri, J.T. and C.J. Dianese,2002Syzygium jambos with stimulatory effects on the germination of Urediniospores of Puccinia psidii.]]>27538542Golovnya, R.B., V.P. Uralets and T.E. Kuzmenko,1976121118121Gouda, Y.G., A.M. Abdel-Baky, K.M. Mohamed, F.M. Darwish, R. Kasai and K. Yamasaki,200620935939Heinrich, G., H.W. Pfeifhofer, E. Stabentheiner and T. Sawidis,200289459469Houghton, P.J., A. Photiou, S. Uddin, P. Shah, M. Browning, S.J. Jackson and S. Retsas,1994Kigelia pinnata against melanoma and renal carcinoma cell lines.]]>60430433Snyder, J.M., S.L. Taylor and J.W. King,199370349354Khatri, L.M. and M.A. Kazi,198133939Lal, S.D. and B.K. Yadar,198337299305Msouthi, J.D. and D. Mangombo,19832694100De Souza, N.J. and W.R. Nes,19698819822Oladele, A.T., G.O. Alade and O.R. Omobuwajo,20112476487Olatunji, A.G. and O. Atolani,2009Kigelia africana: A review.]]>3158164Owolabi, O.J. and E.K.I. Omogbai,2007Kigelia africana (Bignoniaceae).]]>6582585Picerno, P., G. Autore, S. Marzocco, M. Meloni, R. Sanogo and R.P. Aquino,2005Kigelia africana and evaluation of cutaneous irritation in cell cultures and reconstituted human epidermis.]]>6816101614Skaltsa, H.D., C. Demetzos, D. Lazari and M. Sokovic,200364743752Kovats, E.,19584119151932, (In German)Wills, R.B.H., G. Hopkirk and K.J. Scott,198031663666Zhang, D., J.A. Terschak, M.A. Harley, J. Lin and J.D. Hardege,20112011