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Journal of Coordination Chemistry
Year: 2010  |  Volume: 63  |  Issue: 5  |  Page No.: 785 - 793

Two lanthanide luminescent coordination compounds based on 3,5-pyrazoledicarboxylate and oxalic acid

Hong-Yan Wu, Shan-Tang Yue, Ning Wang and Ying-Liang Liu    

Abstract: Two isostructural 3-D complexes [Ln(pdc)(ox)0.5(H2O)2]⋅H2O (Ln = Tb(1), Eu(2); pdc = 3,5-pyrazoledicarboxylate; ox = oxalate) have been synthesized under hydrothermal conditions. Both are characterized by single crystal X-ray diffraction, elemental analysis, and IR. Compounds 1 and 2 possess a 3-D framework with 1-D rectangular channels built from 2-D, brick-like networks, and pdc ligands. The photoluminescence and lifetimes of 1 and 2 in the solid state have been studied.

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