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Journal of Coordination Chemistry
Year: 2009  |  Volume: 62  |  Issue: 12  |  Page No.: 1914 - 1920

One new lanthanide complex with mixed sulfate and oxalate ligands: hydrothermal synthesis, crystal structure, and magnetic properties

Ning Wang, Shan-Tang Yue and Ying-Liang Liu    

Abstract: A new lanthanide complex K[Gd(ox)(SO4)(H2O)] (1) with sulfate and oxalate ligands has been synthesized under hydrothermal conditions. The compound crystallizes in the monoclinic space group P21/c with a = 6.5849(1) Å, b = 8.5660(1) Å, c = 14.7660(2) Å, β = 112.470(1)°, C2H2GdKO9S, M = 398.46, Z = 4, V = 769.66(2) Å3, F(000) = 740, R1 = 0.0199 and ωR = 0.0514. The solid-state DC magnetic susceptibility measurements of 1 revealed antiferromagnetic behavior with an S = 7/2 ground spin state.

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