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Journal of Coordination Chemistry
Year: 2008  |  Volume: 61  |  Issue: 6  |  Page No.: 900 - 906

A new double asymmetric μ1,1-azido bridged binuclear copper(II) complex: crystal structure and magnetic properties

Xuda Wang, Zongwei Li, Yunhe Xu, Licun Li, Daizheng Liao and Zonghui Jiang    

Abstract: A new double asymmetric μ1,1-azido bridged binuclear copper(II) complex, [Cu21,1-N3)2(Him2-py)2(N3)2] (Him2-py = 2-(2’-pyridyl)-4,4,5,5-tetramethylimidazoline-1-hydroxy), has been synthesized and characterized structurally and magnetically. The crystal structure shows this complex is binuclear with copper(II) in a distorted square-pyramidal geometry, bridged by double asymmetric end-on azide ligands. The variable temperature magnetic susceptibility analyses reveal weak antiferromagnetic interaction mediated by the bridge.

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